Exam 3: Tools of the Trade
Exam 1: The Analytical Process20 Questions
Exam 2: Chemical Measurements21 Questions
Exam 3: Tools of the Trade19 Questions
Exam 4: Experimental Error20 Questions
Exam 5: Statistics22 Questions
Exam 6: Quality Assurance and Calibration Methods20 Questions
Exam 7: Chemical Equilibrium20 Questions
Exam 8: Let the Titrations Begin20 Questions
Exam 9: Activity and the Systematic Treatment of Equilibrium20 Questions
Exam 10: Monoprotic Acid-Base Equilibria20 Questions
Exam 11: Polyprotic Acid-Base Equilibria20 Questions
Exam 12: Acid-Base Titrations20 Questions
Exam 13: Edta Titrations20 Questions
Exam 14: Advanced Topics in Equilibrium20 Questions
Exam 15: Fundamentals of Electrochemistry20 Questions
Exam 16: Electrodes and Potentiometry20 Questions
Exam 17: Redox Titrations20 Questions
Exam 18: Electroanalytical Techniques20 Questions
Exam 19: Fundamentals of Spectrophotometry23 Questions
Exam 20: Applications of Spectrophotometry20 Questions
Exam 21: Spectrophotometers20 Questions
Exam 22: Atomic Spectroscopy20 Questions
Exam 23: Mass Spectrometry20 Questions
Exam 24: Introduction to Analytical Separations20 Questions
Exam 25: Gas Chromatography20 Questions
Exam 26: High-Performance Liquid Chromatography20 Questions
Exam 27: Chromatographic Methods and Capillary Electrophoresis20 Questions
Exam 28: Gravimetric and Combustion Analysis20 Questions
Exam 29: Sample Preparation19 Questions
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A 0.1500 M HCl solution was prepared on a day when the temperature was 20oC.What is concentration of the solution when used the next day at 27oC? The density of water is 0.9982071 g/mL at 20oC and 0.9965162 g/mL at 27oC.
Free
(Multiple Choice)
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Correct Answer:
B
A student titrated extracted chloride from a soil sample with 0.1 M silver nitrate.During the titration he performed the following actions while operating the buret. -Washed the buret with silver nitrate solution
-Drained titrant slowly
-Delivered a fraction of a drop near end point
-Read bottom of concave meniscus
-Avoided parallax
-Accounted for graduation thickness in readings
His instructor notes on the student's lab report that the student forgot to____________________ when operating his buret.
Free
(Multiple Choice)
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Correct Answer:
E
____________________ is the liquid from which a substance precipitates or crystallizes.
Free
(Multiple Choice)
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Correct Answer:
D
Which of the following is NOT a good practice when keeping a laboratory notebook?
(Multiple Choice)
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Which of the following statements are TRUE?
I Organic solvents,concentrated acids,and concentrated ammonia should be handled in a fume hood.
II A respirator should be worn when handling organic solvents.
III All containers should be labeled to indicate what they contain.
IV Contact lenses are adequate to protect eyes from liquids and gases in the lab.
(Multiple Choice)
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____________________ is a set of principles intended to help sustain a habitable planet.
(Multiple Choice)
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A researcher dispenses distilled deionized water from a 20-mL volumetric pipet into an empty 8.4376 g weighting bottle.If the total mass of water and weighting bottle is 28.5845 g,what is the volume of the water delivered by the 20-mL pipet? The density of water is 0.9967867 g/mL.
A)20.21 mL
B)20.08 mL
C)28.68 mL
D)19.94 mL
E)19.90 mL
(Essay)
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The mass of the empty receiving vessel used with an analytical balance is the:
(Multiple Choice)
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____________________ is used to convert a precipitate to a known,constant composition.
(Multiple Choice)
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The____________________ fulfills the critical function of reporting what a researcher has done and what they observed,and allows another researcher to repeat their work.
(Multiple Choice)
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On a lab quiz,a student listed the steps to properly use a pipet.Which step is incorrect?
(Multiple Choice)
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____________________ are calibrated to deliver one fixed volume and are____________________ than________________________________________.
(Multiple Choice)
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Which of the following is FALSE regarding volumetric flasks?
(Multiple Choice)
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A student prepares a solution using a 1 L volumetric flask.When he finishes,the meniscus is above the calibration mark on the flask neck.The concentration of the solution is:
(Multiple Choice)
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Which of the responses below are sources of weighing error? I Weighing a sample that is warmer than ambient temperature.
II Cooling a sample in a desiccator prior to weighing.
III Periodically calibrating the balance.
IV The temperature of the balance changing over time.
(Multiple Choice)
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Drying to constant mass is a common gravimetric analysis technique.Which of the statements describe the source of false weights?
I A warm crucible
II Touching the crucible with bare fingers
III Using a microwave oven to dry reagents and crucibles
IV Using a desiccator
(Multiple Choice)
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Which of the statements below is(are)TRUE regarding collecting and storing samples for trace analysis?
I Trace ionic analytes stored in glass are lost by adsorption or contaminated by metals leaching from the glass surface.
II Plastic bottles are recommended to collect and store ionic analyte samples.
III Amber glass bottles are best for collecting and storing aqueous samples of organic materials.
(Multiple Choice)
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____________________ is the upward force exerted on an object in a gaseous or liquid fluid.The mass measured by an analytical balance in air is____________________ its actual mass.
(Multiple Choice)
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